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Fully Automated Hydrogenation Reactor
The equipment is suitable for various hydrogenation reaction scenarios
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Fully Automated Hydrogenation System
Equipment Core Components:
● HPLC Pump: Ensures precise delivery of reactants.
● Dual Gas Feeding System: Adjusts gas mass flow rate for stable supply.
● MC Gas-Liquid Mixer: Enhances gas-liquid mixing and mass transfer efficiency.
● Reaction Chamber: Equipped with solid catalyst for reactions with preheated mixtures.
● Automatic Back Pressure Valve: Maintains stable reaction conditions by regulating back pressure.
| Automatic Micro-reaction Hydrogenation | Gas Feeder | Liquid Feeder | Automatic Back Pressure Valve |
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Advantages Over Traditional Batch High-Pressure Hydrogenation Reactors
● Continuous Operation: Microchannel mixer resolves gas-liquid mixing inhomogeneity and low mass transfer rates.
● High Mass Transfer Efficiency: Leverages plug-flow characteristics for high-selectivity deprotection and significantly reduced reaction time.
Key Advantages
● Full Automation: Automated process control minimizes human error and ensures batch-to-batch consistency.
● Enhanced Hydrogenation Process: Integrated MC gas-liquid mixing module optimizes mixing and mass transfer.
● Inherent Safety: Low in-process liquid holdup with high throughput, supports kilogram-scale customization, and ensures operational safety.
● Compact Design: Space-saving, highly integrated system compatible with fume hood operation.
● Broad Operating Conditions:
● Maximum Reaction Temperature: 200°C，Maximum Reaction Pressure: 10 MPa
● Online Monitoring & Sampling: Equipped with automatic sampling ports and online UV detectors for real-time analysis.
Structure and Parameters
| Model | Hydro-Lab-S10 | Hydro-Lab-H10 | Hydro-Lab-S50 | Hydro-Lab-H50 |
| Material | 316L | HC276 | 316L | HC276 |
| Liquid Holdup | 5.6ml | 150.7ml | ||
| Catalyst Particle Size | 0.2-2mm | |||
| Reaction Pressure | ＜10MPa | |||
| Reaction Temperature | Room temperature-200℃ | |||
| Preheater Temperature | Room temperature-200℃ | |||
| Liquid Feed Flow Rate | 0.02-9.999ml/min | 0.1-50.0ml/min | ||
| Hydrogen Feed Flow Rate | 5-100sccm | 5-100sccm | ||
| Nitrogen Feed Flow Rate | 5-100sccm | 5-100sccm | ||
| Liquid Feed Accuracy | ±2%FS | |||
Catalysts & Technical Support
Customized catalyst selection and sizing recommendations based on client requirements.
| Carbon-loaded Catalysts |  |
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| Palladium on Carbon（Pd/C:Pd%:0.1~30） | Platinum on Carbon（Pt/C:Pt%:0.1~60） | |
| Ruthenium on Carbon（Ru/C:Ru%:0.1~10） | Rhodium on Carbon（Rh/C:Rh%:0.1~10） | |
| Gold on Carbon（Au/C:Au%:0.1~10） | Palladium Hydroxide on Carbon（Pd(OH)/C:Pd%:0.1~30） | |
| Other Support Catalysts | ||
| Alumina-Supported Noble Metal Catalysts | Titania-Supported Metal Catalysts | |
| Molecular Sieve-Supported Noble Metal Catalysts | Inorganic Salt-Supported Noble Metal Catalysts | |
| Silica-Supported Noble Metal Catalysts | Resin-Supported Noble Metal Catalysts | |
| Non-Precious Metal Catalysts | ||
| Copper-Based Catalysts | Nickel-Based Catalysts | |
| Iron-Based Catalysts | Cobalt-Based Catalysts | |
| Manganese-Based Catalysts | Molecular Sieve Catalysts | |
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